Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating

Paria Fazlali; Mahrokh Tahernejad; Leila Biglari; Mahla Eslami

doi:doi:10.11648/j.ijmsa.20241302.11

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Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating

Paria Fazlali, Mahrokh Tahernejad

, Leila Biglari^*, Mahla Eslami

Published in International Journal of Materials Science and Applications (Volume 13, Issue 2)

Received: 7 February 2024 Accepted: 26 February 2024 Published: 2 April 2024

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Abstract

In this research, Polycaprolactone-graphene oxide Nanocomposite coating was synthesized and characterized by Electrospinning on Ti6AL4V alloy. In order to create a uniform coating with optimal thickness, the effective parameters of Electrospinning coating, including solvent, polymer concentration, and bioceramic percentage, were investigated. Also, the cytotoxicity and corrosion tests were evaluated by the electrochemical polarization test method of the created coating in comparisons and different percentages. In order to characterize the coating, a test such as a scanning electron microscope was used. The results showed that as much as the amount of Graphene oxide is increased, the diameter of Nanofibers decreases. The diameter of Polycaprolactone Nanofibers was 1.3 micrometers, which increases to 56.0 micrometers by adding Graphene oxide. The results of the corrosion test showed that the use of Nano composite coating increased the corrosion resistance to the size of the coating. The nanocomposite coating consists of polycaprolactone nanofibers and graphene oxide, which mimics the behavior of the extracellular matrix and improves the biological and antibacterial behavior of the titanium surface. So far, there has been no report on the creation of this fibrous nanocomposite coating on titanium. The results of the cytotoxicity test showed that the use of Nanocomposite coating has effectively reduced the cytotoxicity on the scaffolds. By creating a polycaprolactone-graphene oxide nanofiber composite coating, the biological and antibacterial properties of titanium alloy will be improved and its corrosion resistance will probably change. In this project, the main question is extracting effective parameters in creating a composite coating on titanium surface by electrospinning method and characterizing and biological evaluation of the created coating.

Published in	International Journal of Materials Science and Applications (Volume 13, Issue 2)
DOI	10.11648/j.ijmsa.20241302.11
Page(s)	13-23
Creative Commons	This is an Open Access article, distributed under the terms of the Creative Commons Attribution 4.0 International License (http://creativecommons.org/licenses/by/4.0/), which permits unrestricted use, distribution and reproduction in any medium or format, provided the original work is properly cited.
Copyright	Copyright © The Author(s), 2024. Published by Science Publishing Group

Keywords

Polycaprolactone, Graphene Oxide, MTT Assay, Biomaterial, Electrospinning

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APA Style

Fazlali, P., Tahernejad, M., Biglari, L., Eslami, M. (2024). Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating. International Journal of Materials Science and Applications, 13(2), 13-23. https://doi.org/10.11648/j.ijmsa.20241302.11

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ACS Style

Fazlali, P.; Tahernejad, M.; Biglari, L.; Eslami, M. Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating. Int. J. Mater. Sci. Appl. 2024, 13(2), 13-23. doi: 10.11648/j.ijmsa.20241302.11

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AMA Style

Fazlali P, Tahernejad M, Biglari L, Eslami M. Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating. Int J Mater Sci Appl. 2024;13(2):13-23. doi: 10.11648/j.ijmsa.20241302.11

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@article{10.11648/j.ijmsa.20241302.11,
  author = {Paria Fazlali and Mahrokh Tahernejad and Leila Biglari and Mahla Eslami},
  title = {Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating
},
  journal = {International Journal of Materials Science and Applications},
  volume = {13},
  number = {2},
  pages = {13-23},
  doi = {10.11648/j.ijmsa.20241302.11},
  url = {https://doi.org/10.11648/j.ijmsa.20241302.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20241302.11},
  abstract = {In this research, Polycaprolactone-graphene oxide Nanocomposite coating was synthesized and characterized by Electrospinning on Ti6AL4V alloy. In order to create a uniform coating with optimal thickness, the effective parameters of Electrospinning coating, including solvent, polymer concentration, and bioceramic percentage, were investigated. Also, the cytotoxicity and corrosion tests were evaluated by the electrochemical polarization test method of the created coating in comparisons and different percentages. In order to characterize the coating, a test such as a scanning electron microscope was used. The results showed that as much as the amount of Graphene oxide is increased, the diameter of Nanofibers decreases. The diameter of Polycaprolactone Nanofibers was 1.3 micrometers, which increases to 56.0 micrometers by adding Graphene oxide. The results of the corrosion test showed that the use of Nano composite coating increased the corrosion resistance to the size of the coating. The nanocomposite coating consists of polycaprolactone nanofibers and graphene oxide, which mimics the behavior of the extracellular matrix and improves the biological and antibacterial behavior of the titanium surface. So far, there has been no report on the creation of this fibrous nanocomposite coating on titanium. The results of the cytotoxicity test showed that the use of Nanocomposite coating has effectively reduced the cytotoxicity on the scaffolds. By creating a polycaprolactone-graphene oxide nanofiber composite coating, the biological and antibacterial properties of titanium alloy will be improved and its corrosion resistance will probably change. In this project, the main question is extracting effective parameters in creating a composite coating on titanium surface by electrospinning method and characterizing and biological evaluation of the created coating.
},
 year = {2024}
}

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TY  - JOUR
T1  - Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating

AU  - Paria Fazlali
AU  - Mahrokh Tahernejad
AU  - Leila Biglari
AU  - Mahla Eslami
Y1  - 2024/04/02
PY  - 2024
N1  - https://doi.org/10.11648/j.ijmsa.20241302.11
DO  - 10.11648/j.ijmsa.20241302.11
T2  - International Journal of Materials Science and Applications
JF  - International Journal of Materials Science and Applications
JO  - International Journal of Materials Science and Applications
SP  - 13
EP  - 23
PB  - Science Publishing Group
SN  - 2327-2643
UR  - https://doi.org/10.11648/j.ijmsa.20241302.11
AB  - In this research, Polycaprolactone-graphene oxide Nanocomposite coating was synthesized and characterized by Electrospinning on Ti6AL4V alloy. In order to create a uniform coating with optimal thickness, the effective parameters of Electrospinning coating, including solvent, polymer concentration, and bioceramic percentage, were investigated. Also, the cytotoxicity and corrosion tests were evaluated by the electrochemical polarization test method of the created coating in comparisons and different percentages. In order to characterize the coating, a test such as a scanning electron microscope was used. The results showed that as much as the amount of Graphene oxide is increased, the diameter of Nanofibers decreases. The diameter of Polycaprolactone Nanofibers was 1.3 micrometers, which increases to 56.0 micrometers by adding Graphene oxide. The results of the corrosion test showed that the use of Nano composite coating increased the corrosion resistance to the size of the coating. The nanocomposite coating consists of polycaprolactone nanofibers and graphene oxide, which mimics the behavior of the extracellular matrix and improves the biological and antibacterial behavior of the titanium surface. So far, there has been no report on the creation of this fibrous nanocomposite coating on titanium. The results of the cytotoxicity test showed that the use of Nanocomposite coating has effectively reduced the cytotoxicity on the scaffolds. By creating a polycaprolactone-graphene oxide nanofiber composite coating, the biological and antibacterial properties of titanium alloy will be improved and its corrosion resistance will probably change. In this project, the main question is extracting effective parameters in creating a composite coating on titanium surface by electrospinning method and characterizing and biological evaluation of the created coating.

VL  - 13
IS  - 2
ER  -

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Author Information

Paria Fazlali

Department of Biomedical Engineering, Medical Tehran Branch, Islamic Azad University, Teran, Iran
Mahrokh Tahernejad

Department of Biomedical Engineering, Research and Science Branch, Islamic Azad University, Tehran, Iran

http://orcid.org/0000-0001-5852-5887
Leila Biglari

Department of Biomedical Engineering, University of Shahrekord, Shahrekord, Iran

Contact Email
Mahla Eslami

Department of Biomedical Engineering, Nooshirvani University, Mazandaran, Iran

http://orcid.org/0009-0000-5737-8707

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Plain Text BibTeX RIS

APA Style

Fazlali, P., Tahernejad, M., Biglari, L., Eslami, M. (2024). Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating. International Journal of Materials Science and Applications, 13(2), 13-23. https://doi.org/10.11648/j.ijmsa.20241302.11

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ACS Style

Fazlali, P.; Tahernejad, M.; Biglari, L.; Eslami, M. Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating. Int. J. Mater. Sci. Appl. 2024, 13(2), 13-23. doi: 10.11648/j.ijmsa.20241302.11

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AMA Style

Fazlali P, Tahernejad M, Biglari L, Eslami M. Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating. Int J Mater Sci Appl. 2024;13(2):13-23. doi: 10.11648/j.ijmsa.20241302.11

Copy | Download

@article{10.11648/j.ijmsa.20241302.11,
  author = {Paria Fazlali and Mahrokh Tahernejad and Leila Biglari and Mahla Eslami},
  title = {Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating
},
  journal = {International Journal of Materials Science and Applications},
  volume = {13},
  number = {2},
  pages = {13-23},
  doi = {10.11648/j.ijmsa.20241302.11},
  url = {https://doi.org/10.11648/j.ijmsa.20241302.11},
  eprint = {https://article.sciencepublishinggroup.com/pdf/10.11648.j.ijmsa.20241302.11},
  abstract = {In this research, Polycaprolactone-graphene oxide Nanocomposite coating was synthesized and characterized by Electrospinning on Ti6AL4V alloy. In order to create a uniform coating with optimal thickness, the effective parameters of Electrospinning coating, including solvent, polymer concentration, and bioceramic percentage, were investigated. Also, the cytotoxicity and corrosion tests were evaluated by the electrochemical polarization test method of the created coating in comparisons and different percentages. In order to characterize the coating, a test such as a scanning electron microscope was used. The results showed that as much as the amount of Graphene oxide is increased, the diameter of Nanofibers decreases. The diameter of Polycaprolactone Nanofibers was 1.3 micrometers, which increases to 56.0 micrometers by adding Graphene oxide. The results of the corrosion test showed that the use of Nano composite coating increased the corrosion resistance to the size of the coating. The nanocomposite coating consists of polycaprolactone nanofibers and graphene oxide, which mimics the behavior of the extracellular matrix and improves the biological and antibacterial behavior of the titanium surface. So far, there has been no report on the creation of this fibrous nanocomposite coating on titanium. The results of the cytotoxicity test showed that the use of Nanocomposite coating has effectively reduced the cytotoxicity on the scaffolds. By creating a polycaprolactone-graphene oxide nanofiber composite coating, the biological and antibacterial properties of titanium alloy will be improved and its corrosion resistance will probably change. In this project, the main question is extracting effective parameters in creating a composite coating on titanium surface by electrospinning method and characterizing and biological evaluation of the created coating.
},
 year = {2024}
}

Copy | Download

TY  - JOUR
T1  - Surface Modification of Ti-6Al-4V Alloy by Polycaprolactone-Graphene Oxide Composite Coating

AU  - Paria Fazlali
AU  - Mahrokh Tahernejad
AU  - Leila Biglari
AU  - Mahla Eslami
Y1  - 2024/04/02
PY  - 2024
N1  - https://doi.org/10.11648/j.ijmsa.20241302.11
DO  - 10.11648/j.ijmsa.20241302.11
T2  - International Journal of Materials Science and Applications
JF  - International Journal of Materials Science and Applications
JO  - International Journal of Materials Science and Applications
SP  - 13
EP  - 23
PB  - Science Publishing Group
SN  - 2327-2643
UR  - https://doi.org/10.11648/j.ijmsa.20241302.11
AB  - In this research, Polycaprolactone-graphene oxide Nanocomposite coating was synthesized and characterized by Electrospinning on Ti6AL4V alloy. In order to create a uniform coating with optimal thickness, the effective parameters of Electrospinning coating, including solvent, polymer concentration, and bioceramic percentage, were investigated. Also, the cytotoxicity and corrosion tests were evaluated by the electrochemical polarization test method of the created coating in comparisons and different percentages. In order to characterize the coating, a test such as a scanning electron microscope was used. The results showed that as much as the amount of Graphene oxide is increased, the diameter of Nanofibers decreases. The diameter of Polycaprolactone Nanofibers was 1.3 micrometers, which increases to 56.0 micrometers by adding Graphene oxide. The results of the corrosion test showed that the use of Nano composite coating increased the corrosion resistance to the size of the coating. The nanocomposite coating consists of polycaprolactone nanofibers and graphene oxide, which mimics the behavior of the extracellular matrix and improves the biological and antibacterial behavior of the titanium surface. So far, there has been no report on the creation of this fibrous nanocomposite coating on titanium. The results of the cytotoxicity test showed that the use of Nanocomposite coating has effectively reduced the cytotoxicity on the scaffolds. By creating a polycaprolactone-graphene oxide nanofiber composite coating, the biological and antibacterial properties of titanium alloy will be improved and its corrosion resistance will probably change. In this project, the main question is extracting effective parameters in creating a composite coating on titanium surface by electrospinning method and characterizing and biological evaluation of the created coating.

VL  - 13
IS  - 2
ER  -

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